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dc.contributor.authorPanchadhayee, Rajib
dc.contributor.authorMisra, Anup Kumar
dc.date.accessioned2012-11-23T08:56:08Z
dc.date.available2012-11-23T08:56:08Z
dc.date.issued2009-07-16
dc.identifierFOR ACCESS / DOWNLOAD PROBLEM -- PLEASE CONTACT LIBRARIAN, BOSE INSTITUTE, akc@bic.boseinst.ernet.inen_US
dc.identifier.citationPanchadhayee R and Misra A K (2009) First synthesis of a pentasaccharide repeating unit of the 0- antigenic polysaccharide from enterohemorrhagic E. coli048:H21, Tetrahedron: Asymmetry, 20, 1550- 1555.en_US
dc.identifier.issn0957-4166
dc.identifier.uri1. Full Text Link ->en_US
dc.identifier.urihttp://ac.els-cdn.com/S0957416609004339/1-s2.0-S0957416609004339-main.pdf?_tid=e1d61164-354f-11e2-a6bc-00000aab0f6b&acdnat=1353662979_33a7bb90f00e1853015dac915b516d12en_US
dc.identifier.uri=================================================en_US
dc.identifier.uri2. Scopus : Citation Link ->en_US
dc.identifier.urihttp://www.scopus.com/record/display.url?eid=2-s2.0-67749120488&origin=resultslist&sort=plf-f&src=s&st1=First+synthesis+of+a+pentasaccharide+repeating+unit+of+the+O-antigenic+polysaccharide+from+enterohaemorrhagic+Escherichia+coli&sid=C3_e4E2QzwBcVp0oijnKmUS%3a1210&sot=b&sdt=b&sl=146&s=TITLE-ABS-KEY-AUTH%28First+synthesis+of+a+pentasaccharide+repeating+unit+of+the+O-antigenic+polysaccharide+from+enterohaemorrhagic+Escherichia+coli%29&relpos=0&relpos=0&searchTerm=TITLE-ABS-KEY-AUTH(First%20synthesis%20of%20a%20pentasaccharide%20repeating%20unit%20of%20the%20O-antigenic%20polysaccharide%20from%20enterohaemorrhagic%20Escherichia%20coli)en_US
dc.descriptionDOI : 10.1016/j.tetasy.2009.05.026en_US
dc.description.abstractA concise synthesis of a pentasaccharide as its 4-methoxyphenyl glycoside, found in the O-antigenic polysaccharide of enterohaemorrhagic Escherichia coli O48:H21 has been achieved for the first time in excellent yield. Most of the intermediate steps are high yielding and the stereooutcome of each glycosylation step was excellent. Stereoselective glycosylation and removal of the 4-methoxybenzyl group were achieved in one-pot by tuning the reaction conditions. A late-stage TEMPO-mediated oxidation strategy has been adopted for the oxidation of a primary hydroxyl group to carboxylic acid.en_US
dc.description.sponsorshipCSIR, New Delhi Department of Science and Technology, New Delhi SR/S1/RFPC-06/2006en_US
dc.language.isoenen_US
dc.publisherPERGAMON-ELSEVIER SCIENCEen_US
dc.subjectHEMOLYTIC-UREMIC SYNDROMEen_US
dc.subjectSTRUCTURAL DETERMINATIONen_US
dc.subjectVACCINEen_US
dc.subjectTETRASACCHARIDEen_US
dc.subjectWOS:000268941600016en_US
dc.titleFirst synthesis of a pentasaccharide repeating unit of the O-antigenic polysaccharide from enterohaemorrhagic Escherichia coli O48:H21en_US
dc.title.alternativeTETRAHEDRON-ASYMMETRYen_US
dc.typeArticleen_US


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